It is imperative to establish experimental objectives as a prelude to developing the sampling plan. As a component of development of sampling plan, one must begin by evaluating the environment from which samples will come. To accomplish this goal one must determine the physical and chemical features of the experimental area that includes the basic agents of nutrient supply i.e. soil and water. It contains principles and reactions of chemical analysis, soil sampling and analytical techniques for the determination of physical and chemical parameters of soil and water samples. The book on “Soil and Water Analysis” will be helpful to the Soil Chemists, Agriculture Officers, Specialists and research scholars of soil testing laboratories and other laboratory technicians/assistants.